Search results for "Non destructive"
showing 10 items of 29 documents
Determination of phosphorus by instrumental neutron activation and bremsstrahlung measurement in bone samples
1997
A non destructive method based on the31P(n,γ)32P reaction for the assay of phosphorus in bone samples is described. This method involves a thermal neutron irradiation of 2 minutes in a reactor followed by the measurement of the bremsstrahlung produced by the β− of32P in a Ge-detector surrounded by an anti-Compton shield. Accuracy and precision were tested by analysing the certified NIST 1486 Bone Meal reference material and tri-calcium phosphate (Ca3(PO4)2) samples. The value obtained for the reference material was in good agreement with the certified value and with relative standard deviation of 4.1% the precision was acceptable. The value obtained for Ca3(PO4)2 shows a deviation of −6% fr…
Non-destructive automatic determination of aspect ratio and cross-sectional properties of fibres
2015
A novel method for computerised estimation of the aspect ratio distribution and various cross-sectional geometrical properties of fibres in short-fibre reinforced composites is proposed. The method, based on X-ray micro-computed tomography, is non-destructive and does not require user intervention. Based on results on specially fabricated model material, the accuracy and precision of the method seems adequate. The method is applied in analysing a manufacturing process of wood fibre reinforced thermoplastic composite. The results indicate a significant decrease of the aspect ratio of fibres during the processing steps. Finally, the feasibility of the method is assessed by estimating paramete…
Preliminary analysis of Palaeolithic black pigments in plaquettes from the Parpalló cave (Gandía, Spain) carried out by means of non-destructive tech…
2013
Abstract Parpallo cave (Gandia, Spain) is one of the most important Palaeolithic sites in the Spanish Mediterranean region. It is characterized by a mobiliary art whose archaeological sequence covers a dilated period (26,000–11,000 BP) and includes plaquettes decorated with black and different shades of red and yellow pigments. The aim of this paper is to present the results of analyses of the nature of black pigments used in the decoration of Parpallo plaquettes. The analyses were carried out by a non-destructive technique, by means of EDXRF. Furthermore, a colorimetric data bank has been created for conservation purposes. EDXRF measurements directly identify the use of manganese black pig…
Full-scale validation of bio-recycled asphalt mixtures for road pavements
2019
Abstract Recycling of asphalt has become a well-established practice in many countries, however the road pavement industry remains a bulk consumer of extracted raw materials. Novel solutions that find root in circular economy concepts and life-cycle approaches are needed in order to enable optimisation of infrastructure resource efficiency, starting from the design stage and spanning the whole value chain in the construction sector. Itis within this framework that the present study presents a full-scale validation of asphalt mixtures specifically designed to ensure durability of flexible road pavements and at the same time enabling the reuse of reclaimed asphalt pavement (RAP) through the i…
Development of a dielectric spectroscopy technique for the determination of apple (Granny Smith) maturity
2010
Abstract Dielectric measurements of apple were done during its maturity in order to find relations with apple physiological compounds (sugar content, malic acid). An Agilent 85070E open-ended coaxial probe connected to an Agilent E8362B vector network analyzer were used in these experiments. All determinations were made at 30 °C from 500 MHz to 20 GHz. These assays were performed in order to consider the potential use of dielectric spectroscopy for determining the state of fruit maturity. Good correlations among apples Thiault Index with a new defined Dielectric Maturity Index were found. The Dielectric Maturity Index was related to loss factor at two punctual frequencies (0.5 GHz and dipol…
Field non-destructive determination of nectarine quality under deficit irrigation
2021
This study investigated the effects of deficit irrigation (DI) at different fruit growth stages and tree orientation on fruit quality of ‘September Bright’ nectarines (Prunus persica L. Batsch). Control trees were fully irrigated throughout the entire fruit development period, whereas deficit irrigation was supplied at fruit growth stage I (cell division, DI-I), II (pit hardening, DI-II), IIIa (cell expansion, DI-IIIa) and IIIb (fruit maturation, DI-IIIb). Non-destructive measurements of fruit maturity and quality were carried out using portable devices based on near-infrared spectrometry and pigment fluorescence on west- and east-oriented trees of an Open Tatura system. Chlorophyll degrada…
Portable non invasive analyses for Cultural Heritage
2014
The requirements that the scientific analyses for Cultural Heritage must have are: nondestructive and noninvasive, multielemental, sensitive, reliable and sufficiently rapid, able to carry out measurements in situ on objects of all types, and to deduce information practically on-line. Among the techniques that fulfill these requirements we find: multispectral imaging, portable EDXRF, Raman and UV-VIS-NIR spectrometry. In this paper we are going to show some cases in which it will appear clear the necessity of the correct order with which applying the non invasive techniques and what data of each of them it is necessary to understand in situ to obtain the maximum of the subsequent scientific…
Machine learning at the interface of structural health monitoring and non-destructive evaluation
2020
While both non-destructive evaluation (NDE) and structural health monitoring (SHM) share the objective of damage detection and identification in structures, they are distinct in many respects. This paper will discuss the differences and commonalities and consider ultrasonic/guided-wave inspection as a technology at the interface of the two methodologies. It will discuss how data-based/machine learning analysis provides a powerful approach to ultrasonic NDE/SHM in terms of the available algorithms, and more generally, how different techniques can accommodate the very substantial quantities of data that are provided by modern monitoring campaigns. Several machine learning methods will be illu…
XRF analysis to identify historical photographic processes: The case of some Interguglielmi Jr.’s images from the Palermo Municipal Archive
2017
Abstract In the early period, even though professional photographers worked with similar techniques and products, their artistic and commercial aims determined different choices and led them to follow different, often personal, recipes. For this reason, identification of the techniques through date and name of the photographer or through some visual features like colour, tonality and surface of the image layer, often needs further investigation to be proved. Chemical characterization, carried out in a non or micro destructive way, can be crucial to provide useful information about the original composition, degradation process, realization technique, in obtaining an indirect dating of the ph…
Energy dispersive X-ray diffraction potentiality in the field of cultural heritage: simultaneous structural and elemental analysis of various artefac…
2007
The applicability of an Energy Dispersive X-ray Diffractometer to some technical questions in the field of Cultural Heritage is presented. This diffractometer, equipped with a white source, has been utilized for the structural and elemental analysis of some items having different nature. Given its design, the instrument allows to collect data from samples as big as a book or a little more. Samples, without collection of any portion and without any preliminary preparation, have been placed in the instrument and spectra have been collected in a wide energy range that contains X-ray fluorescence and diffraction features. In all cases, data acquired in air and in a non destructive way were reli…